Abstract:
The electrochemical anodization of titanium has received a lot of attention in recent years, especially for its application for biomedical purposes, offering a biocompatible titanium oxide with architecture of a large energy surface, and highly controllable nanoscale characteristics.In this work, TiO2 layers were synthesized on a well-polished titanium surface, by the anodizing technique, under a voltage of 20 V, for 15, 30 and 45 minutes respectively, using as specific electrolyte: 1M CH3COOH /1M Na2SO4/0.5 Wt% NaF.Interfacial integrity and variation of elemental composition along the interface were studied by scanning electron microscopy (SEM), equipped with an energy dispersive X-ray analyzer (EDX). Electrochemical behaviour was studied both by measuring the evolution of open circuit potential (OCP), by electrochemical impedance spectroscopy (EIS), and by linear polarization (LP) in Hank's solution as a physiological environment. [..]
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