NANOCOMPOSITES OF ZNO-DECORATED HPHT NANODIAMOND AS A PERSPECTIVE GREEN PHOTOCATALYSTS

1 MICOVA Julia
Co-authors:
1 KOSUTOVA Natalia 2,3 JERIGOVA Monika 4 REMES Zdenek
Institutions:
1 Slovak Academy of Sciences, Institute of Chemistry, Bratislava, Slovakia, EU, chemjumi@savba.sk
2 International Laser Centre, Bratislava, Slovakia, EU
3 Department of Physical and Theoretical Chemistry, Faculty of Natural Sciences, Comenius University, Mlynska dolina, Bratislava, Slovakia, EU
4 Czech Academy of Sciences, Institute of Physics, Prague, Czech Republic, EU
Conference:
16th International Conference on Nanomaterials - Research & Application, OREA Congress Hotel Brno, Czech Republic, EU, October 16 - 18, 2024
Proceedings:
Proceedings 16th International Conference on Nanomaterials - Research & Application
Pages:
171-176
ISBN:
978-80-88365-24-2
ISSN:
2694-930X
Published:
28th February 2025
Metrics:
27 views / 14 downloads
Abstract

Electrical and optical properties of zinc oxide, in particular the relatively wide direct band gap of ~3.3 eV predetermines ZnO as a photocatalytic material at room temperature. ZnO itself is non-toxic and the hydrothermal growth method we use to prepare its nanostructures is environmentally friendly. These facts contribute to the attractiveness of this material. Recently, we have focused on studying the influence of doping or of plasma surface treatment on the photocatalytic efficiency of ZnO. However, the main drawbacks are the high recombination rate of charge carriers and the poor in capturing visible light in a narrow spectral range. The solution is the use of ZnO as part of nanocomposites. In the past, ZnO-detonation nanodiamons (DND) composites were studied. The disadvantage of DND is the formation of clusters of different sizes, therefore we focused our attention on the use of HPHT nanodiamonds (NDs). We modified the surface of commercial HPHT NDs by oxidation in order to increase the concentration of hydroxyl-, carbonyl- and carboxyl- functional groups. The resulting ZnO-HPHT NDs composites were synthesized using a dehydration-condensation process between oxygen-containing functional groups on the NDs surface and hydroxyl groups on the ZnO surface. The prepared nanocomposites were characterized by SEM, EDX spectroscopy and secondary ion mass spectrometry (SIMS) and tested by photocatalytic dye degradation.

Keywords: HPHT NDs, ZnO, nanocomposites, photocatalyst, photocatalytic oxidation

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