SPINEL FERRITES NANOPARTICLES FOR ALLOY STEEL PROTECTIVE LAYERS

1 OCHMANN Martin
Co-authors:
1 LINDERHOF Fredericus M. A. 1,2 MACHALA Libor
Institutions:
1 Department of Experimental Physics, Faculty of Science, Palacký University, Olomouc, Czech Republic, EU
2 Regional Centre of Advanced Technologies and Materials, Palacký University, Olomouc, Czech Republic, EU
Conference:
12th International Conference on Nanomaterials - Research & Application, Brno, Czech Republic, EU, October 21 - 23, 2020
Proceedings:
Proceedings 12th International Conference on Nanomaterials - Research & Application
Pages:
208-213
ISBN:
978-80-87294-98-7
ISSN:
2694-930X
Published:
28th December 2020
Proceedings of the conference were published in Web of Science and Scopus.
Metrics:
873 views / 444 downloads
Abstract

Covering layers might have very important role in improving performance of many mechanical parts. These layers are usually designed to protect a substrate from the environment and enhance mechanical properties such as hardness. Blackening is a classical approach that is very demanding on resources. This process is based on the alkalisation of surface atoms and the transformation of formed hydroxides to oxides. Such an approach inspired us to carry out experiments resulting in preparation of protective layers with similar properties, by using stoichiometric spinel ferrite nanoparticles (MeFe2O4). Thus mechanical parts were covered with ferrite nanoparticles and heated in a furnace. Ferrite samples, which were used as precursor for the preparation of layers, were analysed with X-ray powder diffraction, energy dispersive X-ray spectroscopy and 57Fe Mössbauer spectroscopy. The samples were analysed with ultrasonic hardness test, electron microscopy, and Mössbauer spectroscopy. The protection layers showed a higher hardness compared to untreated parts.

Keywords: Spinel ferrites, protective layer, Mössbauer spectroscopy, hardness test

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