TESTING OF CORROSION BEHAVIOR OF NICKEL ALLOYS AT HIGH TEMPERATURES IN MOLTEN SALTS

1 REJKOVÁ Jana
Co-authors:
1 KUDRNOVÁ Marie
Institution:
1 UCT - University of Chemistry and Technology, Prague, Czech Republic, EU, petruj@vscht.cz, hubickom@vscht.cz
Conference:
31st International Conference on Metallurgy and Materials, Orea Congress Hotel Brno, Czech Republic, EU, May 18 - 19, 2022
Proceedings:
Proceedings 31st International Conference on Metallurgy and Materials
Pages:
762-766
ISBN:
978-80-88365-06-8
ISSN:
2694-9296
Published:
1st November 2022
Proceedings of the conference were published in Web of Science and Scopus.
Metrics:
399 views / 191 downloads
Abstract

The use of salt mixtures properties is considered in many future technologies, such as energy storage or medium for nuclear reactors. The key question is to choose a suitable construction material for these devices operating at high temperatures in a corrosive environment. Nickel alloys show high corrosion resistance at high exposure temperatures, and literary sources also describe resistance in the environment of fluoride salts. This work verified the corrosion behavior of two nickel alloys in molten chloride salts. Nickel-based superalloys Hastelloy C22 and MoNiCr were tested in a mixture of chloride salts LiCl - KCl (58.2 - 41.8 wt%). Alloys samples were heated in salt melts for 500 h at 440 °C in an inert atmosphere of argon. After removal, they were analyzed gravimetrically, the composition of the surface layers by the XPS and cross-section of samples using SEM. The gravimetric evaluation showed no significant changes after exposure. This was also confirmed by SEM and XPS results, which demonstrate the formation of very thin layers of nickel and chromium oxides up to 1 µm thick.

Keywords: Nickel alloy, molten chloride salts, corrosion, nuclear reactor

© This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

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