MATERIALS BASED ON QUINOLINE SULFONAMIDE - METALS WITH ANTIMICROBIAL ACTIVITY AND THEIR X-RAY CHARACTERISATION

2 DIACONU Dumitrela
Co-authors:
2 MANGALAGIU Violeta 1 CIORTEANU Roxana 1,2 MANGALAGIU Ionel I.
Institutions:
1 Alexandru Ioan Cuza University of Iasi, Faculty of Chemistry, Iasi, Romania, EU, ionelm@uaic.ro
2 Alexandru Ioan Cuza University of Iasi, Institute of Interdisciplinary Research – CERNESIM Center, Iasi, Romania, EU, violeta.mangalagiu@uaic.ro, cucu.dumitrela@yahoo.com
Conference:
31st International Conference on Metallurgy and Materials, Orea Congress Hotel Brno, Czech Republic, EU, May 18 - 19, 2022
Proceedings:
Proceedings 31st International Conference on Metallurgy and Materials
Pages:
739-744
ISBN:
978-80-88365-06-8
ISSN:
2694-9296
Published:
1st November 2022
Proceedings of the conference were published in Web of Science and Scopus.
Metrics:
395 views / 210 downloads
Abstract

Quinoline sulfonamide complexes with different metals represent a new class of materials of great interest especially for their fotoluminiscent and biological activity (mostly antibacterial and antifungal activity). The emphasis of this work was to synthesize, characterize through X-ray and determine the antibacterial and antifungal proprieties of newly materials for medicinal chemistry applications based on Quinoline Sulfonamide Complexes Metals (QSCM). The synthesis of the QSCM materials is straight and efficient, in two steps: acylation of aminoquinoline followed by complexation with M2+ metal (Zn2+, Cd2+, Co2+, Cu2+). The synthesized quinoline sulfonamide complexes M2+ metals were characterized by X-ray diffraction on single crystal and by FTIR and NMR spectroscopy. The X-ray spectra prove unambiguously the structure of complexes, e.g for the Zn (II) complex crystallize in the monoclinic P21/n space group type, with a= 1.21602(5) nm, b = 1.55478(5) nm, c = 1.61786(6) nm, α = 90°, β = 106.007(2)°, γ = 90°, V= 2.9402(19) nm3and Z = 4.Sulfonamide acts as bidentate ligand trough Zn-Nquinoline and Zn-Nsulfonamide bonds, with atetrahedral coordination environment for Zn2+. The QSCMM2+ complexes were tested for their antibacterial and antifungal activity, having a good antibacterial activity against gram positive germStaphylococcus aureus,andgram negative germ Escherichia coli, and an excellent antifungal activity against fungus Candida albicans.

Keywords: X-Ray, quinoline sulfonamide complexes, M2+ transitional metals, antibacterial, antifungal

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