EVOLUTION OF THE MICROSTRUCTURE AND MAGNETIC PROPERTIES OF MELT SPUN FE2NIAL ALLOY DURING AGING

1 Menushenkov Vladimir
Co-authors:
1 Gorshenkov Mikhail 1 Shchetinin Igor 1 Savchenko Elena
Institution:
1 National University of Science and Technology “MISiS”, Moscow, Russian Federation, menushenkov@gmail.com
Conference:
24th International Conference on Metallurgy and Materials, Hotel Voronez I, Brno, Czech Republic, EU, June 3rd - 5th 2015
Proceedings:
Proceedings 24th International Conference on Metallurgy and Materials
Pages:
1346-1351
ISBN:
978-80-87294-58-1
ISSN:
2694-9296
Published:
12th January 2015
Proceedings of the conference were published in Web of Science and Scopus.
Metrics:
378 views / 159 downloads
Abstract

A microcrystalline Alni alloy with the nominal composition Fe51.1Ni23.5Al23.7Si1.7 was prepared by melt-spinning. Detailed studies of the spinodal decomposition (SD), microstructure and magnetic properties of the ribbons subjected to isothermal aging at Tag = 500-780 °C are reported. TEM investigations of the decomposition of the solid solution (β2 → β + β2) after melt-spinning and aging have revealed several types of decomposition products. As prepared melt spun ribbons show zone structure and antiphase domain (APD) boundaries inside grains. Aging at 500-600 °C led to the coarsening of the zone microstructure and to the appearance of discontinuous precipitates (DP) (β + β2 → β' + β'2) at grain boundaries. Aging at higher than 650 °C causes the formation of a modulated microstructure instead of a zone microstructure inside grains and coarsening of DP products. As prepared ribbons reveal soft magnetic properties (Hc = 480 Am-1). The maximum coercivity Hc = 20 kAm-1 was obtained for the ribbons aged at 700 °C. MFM method was used to image the magnetic microstructure of melt spun Alni ribbons subjected to aging.

Keywords: Alni alloy, melt-spinning, aging, antiphase domains, discontinuous precipitates

© This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

Scroll to Top