STRUCTURAL CHANGES OF PVD COATED CR-NI STEEL AFTER HEAT LOAD

1 KRUM Stanislav
Co-authors:
1 HORNÍK Jakub 1 TONDL David 2 PEŠLOVÁ Františka 1 PUCHNIN Maxim 1 ANISIMOV Evgenyi
Institutions:
1 Czech Technical University in Prague, Faculty of Mechanical Engineering, Department of Material Engineering, Prague, Czech Republic, EU, s.krum@seznam.cz, jakub.hornik@fs.cvut.cz, tondl@ipp.cas.cz, maxim.puchnin@fs.cvut.cz, evgenyi.anisimov@fs.cvut.cz
2 Alexander Dubcek University of Trencin, Faculty of Industrial Technologies in Puchov, Puchov, Slovakia, EU, frantiska.peslova@fpt.tnuni.sk
Conference:
23rd International Conference on Metallurgy and Materials, Hotel Voronez I, Brno, Czech Republic, EU, May 21 - 23, 2014
Proceedings:
Proceedings 23rd International Conference on Metallurgy and Materials
Pages:
902-907
ISBN:
978-80-87294-52-9
ISSN:
2694-9296
Published:
18th June 2014
Proceedings of the conference were published in Web of Science and Scopus.
Metrics:
336 views / 138 downloads
Abstract

The paper deals with evaluation of PVD functionally graded coatings based on Cr-Al-N, TiN and Ti-Al-N. Coatings were deposited in the following combinations: CrAl/CrAlN, Cr/CrN/CrAlN, nitriding/Cr/CrN/CrAlN, nitriding/TiN/AlTiN and nitriding/AlTi/AlTiN. As main criteria for coatings properties and quality comparison methods of scratch test and nanohardness measurement were selected. Subsequently, coatings CrAlN and TiN were designed as protection against high temperature oxidation of Cr-Ni steel (X16CrNiSi25-20) exposed to the temperature of 850 °C for 6 and 12 hours duration. Detailed microstructural analysis of the coating - substrate interface including EDS microanalysis of the elements distribution in the coating and the substrate was performed. Scratch test of selected coating after heat exposure was carried out in order to determine adhesion. From simulated tests it is evident that PVD coating CrAlN fulfils the role of protection. In the case of TiN there occurred intensive subsurface degradation of the coating connected with decohesion and subsequent cracking off the coating.

Keywords: PVD coating, FGM, CrNi austenitic steel, heat load, CrAlN

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